BAMB-4_LCMS_14630_MedChemExpress

MS Report from Instrument: LCMS-03 File ..ata\\20170920\\20170920-1\\CPK2017-920-14630.D Tgt Mass (CHM): Injection Date : 20 Sep 17 6:28 pm +0800 Seq. Line : 50 Sample Name : CPK2017-920-14630 Location : P1-F-09 Acq. Operator : SYSTEM Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\LCMS03\\Data\\20170920\\20170920-1\\1-POS-3MIN.M Analysis Method : D:\\LCMS03\\Data\\20170920\\20170920-1\\1-POS-3MIN.M Catalog No : HY-16694 Batch#14630 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C DAD1 A, Sig=214,4 Ref=off1.8321.419mAU1.1621.7271.757500000.5 DAD1 B, Sig=254,4 Ref=offmAU1.1721.7571.4041.5500000.5 ELS1 A, ELSD SignalmV100000.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70600000040000002000000000.51 Ion 252.3, MSD1 252.3,Target Mass 252.3 Positive, EIC=252:253100005000000.511.522.5min Integration Results for DAD1 A, Sig=214,4 Ref=off1.522.0602.5min1.51.86022.5min111.9262.2121.51.83222.5min1.9242.2121.51.722.5min RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.16 0.02 3.95 0.03 0.34 325 1.42 0.01 2.56 3.22 0.22 233 1.73 0.01 0.21 0.29 0.02 105 1.76 0.01 0.65 0.70 0.06 105 1.83 0.02 1142.76 1111.32 99.02 253 1.93 0.03 1.05 0.65 0.09 527 2.21 0.02 2.85 3.16 0.25 105 Integration Results for DAD1 B, Sig=254,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.17 0.02 2.48 2.73 0.22 325 1.40 0.01 0.78 0.05 0.07 233 1.59 0.01 0.46 -0.05 0.04 233 1.76 0.01 0.21 0.26 0.02 105 1.83 0.01 1102.02 1083.30 99.32 253 1.92 0.01 0.35 0.43 0.03 527 2.21 0.02 3.29 3.17 0.30 105LCMS-03 9/21/2017 10:32:12 SYSTEMPage1 of4MS Report from Instrument: LCMS-03 Integration Results for MSD1 TIC, MS File RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.86 0.06 25972462.00 6358146.00 100.00 253LCMS-03 9/21/2017 10:32:12 SYSTEMPage2 of4MS Report from Instrument: LCMS-03Ret. Time: 1.86 <<<< POSITIVE SPECTRA >>>> ES-API Positive253.1400000300000254.1275.1100000105.1179.1312.10100200300400500600700800900m/z529.2528.2200000527.2LCMS-03 9/21/2017 10:32:12 SYSTEMPage3 of4MS Report from Instrument: LCMS-03 *** End of Report ***LCMS-03 9/21/2017 10:32:12 SYSTEMPage4 of4