Data File D:\\AGLIENT 1260\\DATA\\20150402\\20150402 2015-04-02 09-08-41\\CPK2015-402-04504.DSample Name: CPK2015-402-04504=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 68Acq. Instrument : HY-LCMS-02 Location : P1-A-06Injection Date : 4/2/2015 3:52:46 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20150402\\20150402 2015-04-02 09-08-41\\100-1000MS+3MIN- 1.5_(0.02%FA).MLast changed : 4/2/2015 9:08:41 AM by Li Shan(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\DATA\\20150401\\20150401 2015-04-01 09-07-02\\HY-003G_6- H01RS01(RP-HPLC).M (Sequence Method)Last changed : 4/2/2015 3:59:59 PM by Li Shan(LCMS-02) (modified after loading)Method Info : Negtive,Positive,MS:100-1000,Column ID:A-RP-108,30℃ Catalog No : HY-10460 Batch#04504 A-RP-132 Additional Info : Peak(s) manually integrated DAD1 B, Sig=214,4 Ref=off (D:\\AGLIENT...0\\DATA\\20150402\\20150402 2015-04-02 09-08-41\\CPK2015-402-04504.D) 1.810 1.718 1.551 1.973mAU70060050040030020010000.511.522.53min ===================================================================== Area Percent Report ===================================================================== Sorted By : SignalMultiplier : 1.0000Dilution : 1.0000Do not use Multiplier & Dilution Factor with ISTDs Signal 1: DAD1 B, Sig=214,4 Ref=off Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %----|-------|----|-------|----------|----------|--------| 1 1.551 MM 0.1298 2.87572 3.69218e-1 0.1249 2 1.718 MM 0.0362 3.10538 1.42788 0.1349 3 1.810 MM 0.0444 2287.73608 859.35455 99.4022 4 1.973 MM 0.0594 7.778 2.18251 0.3379 Totals : 2301.49365 863.33417 ===================================================================== *** End of Report ***HY-LCMS-02 4/2/2015 4:00:01 PM Li Shan(LCMS-02)Page 1 of 1
Data File D:\\AGLIENT 1260\\DATA\\20150402\\20150402 2015-04-02 09-08-41\\CPK2015-402-04504.DSample Name: CPK2015-402-04504HY-10460-20110901A-RP-132=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 68Acq. Instrument : HY-LCMS-02 Location : P1-A-06Injection Date : 4/2/2015 3:52:46 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20150402\\20150402 2015-04-02 09-08-41\\100-1000MS+3MIN- 1.5_(0.02%FA).MLast changed : 4/2/2015 9:08:41 AM by Li Shan(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\DATA\\20150401\\20150401 2015-04-01 09-07-02\\HY-003G_6- H01RS01(RP-HPLC).M (Sequence Method)Last changed : 4/2/2015 4:01:43 PM by Li Shan(LCMS-02) (modified after loading)Method Info : Negtive,Positive,MS:100-1000,Column ID:A-RP-108,30℃ Catalog No : HY-10460 Batch#04504 A-RP-132 Additional Info : Peak(s) manually integrated MSD1 TIC, MS File (D:\\AGLIENT 1260\\DATA\\20150402\\20150402 2015-04-02 09-08-41\\CPK2015-402-04504.D) ES-API, Pos, Sc 1.81450000040000030000020000010000000.511.522.53min HY-LCMS-02 4/2/2015 4:01:44 PM Li Shan(LCMS-02)Page 1 of 2
Data File D:\\AGLIENT 1260\\DATA\\20150402\\20150402 2015-04-02 09-08-41\\CPK2015-402-04504.DSample Name: CPK2015-402-04504MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 50 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts. Reportable Ion Abundance: > 10%. Retention Mol. WeightTime (MS) MS Area or Ion 1.814 19672 507.70 I 506.80 I*MSD1 SPC, time=1.798:1.835 of D:\\AGLIENT 1260\\DATA\\20150402\\20150402 2015-04-02 09-08-41\\CPK2015-402-04504.D ES-API100806040200100200300400500600700m/z 506.8Max: 305835 *** End of Report ***HY-LCMS-02 4/2/2015 4:01:44 PM Li Shan(LCMS-02) 508.8 507.7Page 2 of 2